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Sodium Saccharin

CERTIFICATE  OF  ANALYSIS

                       DATE:15/02/2016 

SODIUM SACCHARIN 20-40MESH                    BATCH NO.20160215

QUANTITY:16.2000KGS                              DATE OF MFG. : FEB,2016    

PACKING25KG PLASTIC BAG                     DATE OF EXPIRY:FEB,2021   

MOLECULAR FORMULAR :C7H4O3NSNa.2H2O        MOLECULAR WT. 241.21

ITEMS

      STANDARD

       RESULTS

Identification

Positive

Complies

Melting point of   insolated saccharin ℃

226-230

228.4 –228.6

Appearance

Colorless   Crystals or White Crystalline Power

Complies

Content  %

99.0-101.0

99.56

Loss on drying %

≤15

13.95

Ammonium salts  ppm

≤25

16 ppm

Arsenic  ppm

≤3

1.3ppm

Benzoate and   salicylate

No precipitate or   violet color appears

Complies

Heavy metals  ppm

≤10

6.5 ppm

Free acid or alkali

Complies with BP   /USP

Complies

Readily   carbonizable substances

Not more intensely   colored than reference

Complies

P-toluene   sulfonamide

≤10ppm

7ppm

O-toluene   sulfonamide

≤10ppm

8ppm

Selenium  ppm

≤30

15ppm

Related substance

Complies with DAB

Without

Clarity and color   solution

Color less clear

Color less clear

Organic volatiles

Complies with BP

Without

PH value

Complies with   BP/USP

7.3

Benzoic   acid-sulfonamide

≤25ppm

16ppm

 

 

 

MICROBIAL   COUNTS

Total count of   bacteria

Not more than 1000/gm.

Total moulds

Not more than 100/gm.

Total yeasts

Not more than 100/gm.

Enterobacteriaceae:


-- Salmonella

Not detectable/gm.

-- E. coli

Not detectable/gm.

-- Others

Not more than 100/gm.

Pseudomonas aeruginosa

Not detectable/gm.

Staph. aureu

Not detectable/gm.

DETERMINATION: Complies withBP2008/USP32

SHELF LIFE: 5 Years/MAX 10 Years.


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